6RSK
Cytochrome c co-crystallized with 20 eq. sulfonato-calix[8]arene and 15 eq. spermine - structure II
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-01 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.97624 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 100.459, 100.459, 89.539 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.840 - 2.310 |
R-factor | 0.185 |
Rwork | 0.183 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6gd9 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.035 | 2.346 |
High resolution limit [Å] | 2.306 | 2.306 |
Rmerge | 0.196 | 1.871 |
Rpim | 0.039 | 0.358 |
Number of reflections | 20779 | 1006 |
<I/σ(I)> | 13.4 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 25.9 | |
CC(1/2) | 0.993 | 0.748 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M HEPES pH 7.5, 0.15 M NaCl, 2.2 M Ammonium sulfate, 0.04 M sulfonato-calix[8]arene, 0.03 M spermine |