6RCY
CRYSTAL STRUCTURE OF FK1 DOMAIN OF FKBP52 IN COMPLEX WITH A BIO-INSPIRED HYBRID FLUORESCENT LIGAND
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-25 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.976 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 52.960, 52.960, 237.860 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.030 - 2.300 |
R-factor | 0.22 |
Rwork | 0.218 |
R-free | 0.24400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1n1a |
RMSD bond length | 0.009 |
RMSD bond angle | 1.170 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.800 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmeas | 0.127 | 2.405 |
Number of reflections | 9583 | 1440 |
<I/σ(I)> | 15.6 | |
Completeness [%] | 99.6 | |
Redundancy | 20.3 | |
CC(1/2) | 0.999 | 0.780 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.8M potassium phosphate, 0.8M sodium phosphate, 0.1M HEPES, pH 7.5 |