6R2Q

Structure of the Mtr complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-09-10
Detector	DECTRIS PILATUS 300K
Wavelength(s)	0.97624
Spacegroup name	C 2 2 21
Unit cell lengths	212.042, 234.165, 99.192
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	73.250 - 2.697
R-factor	0.2258
Rwork	0.224
R-free	0.25730
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	SHELXDE
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	106.021	2.814
High resolution limit [Å]	2.697	2.697
Rmerge	0.091
Rpim	0.042
Number of reflections	49758	2489
<I/σ(I)>	13.3	2.6
Completeness [%]	94.1	97.1
Redundancy	5.5	4.7
CC(1/2)	0.997	0.908

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		289	0.1 M Bis-Tris, 0.01 M LDAO, 0.4 M Calcium chloride, 40 % MPD