6R2Q
Structure of the Mtr complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-09-10 |
| Detector | DECTRIS PILATUS 300K |
| Wavelength(s) | 0.97624 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 212.042, 234.165, 99.192 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 73.250 - 2.697 |
| R-factor | 0.2258 |
| Rwork | 0.224 |
| R-free | 0.25730 |
| Structure solution method | SAD |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | SHELXDE |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 106.021 | 2.814 |
| High resolution limit [Å] | 2.697 | 2.697 |
| Rmerge | 0.091 | |
| Rpim | 0.042 | |
| Number of reflections | 49758 | 2489 |
| <I/σ(I)> | 13.3 | 2.6 |
| Completeness [%] | 94.1 | 97.1 |
| Redundancy | 5.5 | 4.7 |
| CC(1/2) | 0.997 | 0.908 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Bis-Tris, 0.01 M LDAO, 0.4 M Calcium chloride, 40 % MPD |
