6R0E
Structure of F11TCR in complex with DR1 MHC Class II presenting PKYVKQNTLKLAT
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-22 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97623 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 132.280, 184.900, 50.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 92.450 - 1.910 |
Rwork | 0.205 |
R-free | 0.23320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fyt |
RMSD bond length | 0.011 |
RMSD bond angle | 1.709 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 92.460 | 1.960 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.078 | 1.260 |
Rmeas | 0.084 | 1.354 |
Rpim | 0.031 | 0.491 |
Number of reflections | 96543 | 7001 |
<I/σ(I)> | 14.1 | |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 7.2 | 7.4 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 291 | 0.1 M Na Cacodylate, 0.2 M NH4 SO4, 15 % PEG 8000 |