6QYH
Structure of Apo HPAB from E.coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97857 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 189.280, 189.280, 163.530 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.450 - 1.940 |
R-factor | 0.167 |
Rwork | 0.166 |
R-free | 0.18400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4oo2 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.960 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.6.0) |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.400 | 2.010 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.161 | 3.410 |
Rmeas | 0.164 | 3.478 |
Rpim | 0.032 | 0.677 |
Number of reflections | 127313 | 12389 |
<I/σ(I)> | 13.3 | 1 |
Completeness [%] | 99.9 | 98.8 |
Redundancy | 26.13 | 25.84 |
CC(1/2) | 0.999 | 0.472 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | HEPES 0.1M pH 7.5 PEG 400 30% (w/v) CaCl2 0.2M MgCl2 0.1M |