6QP9
Drosophila Semaphorin 1a, extracellular domains 1-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-01-27 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 32 |
Unit cell lengths | 99.476, 99.476, 150.131 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.738 - 3.600 |
R-factor | 0.2934 |
Rwork | 0.287 |
R-free | 0.32260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fkk |
RMSD bond length | 0.002 |
RMSD bond angle | 0.575 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.740 | 3.820 |
High resolution limit [Å] | 3.600 | 3.600 |
Rmerge | 0.233 | |
Number of reflections | 19133 | |
<I/σ(I)> | 5 | |
Completeness [%] | 97.0 | |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293.15 | 0.1 M Tris-HCl (pH 8.0), 0.2 M ammonium sulphate, 25% PEG 3350 |