6QIG
Metalloproteinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-14 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.969 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 87.532, 87.532, 407.342 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.200 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.167 | |
Number of reflections | 45840 | |
<I/σ(I)> | 11.7 | |
Completeness [%] | 99.3 | |
Redundancy | 12.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 35% (v/v) pentaerythritol ethoxylate, 200 mM CaCl2, 100 mM HEPES, pH 6.5 |