6Q2X
TEAD4 (216-434) COMPLEXED WITH YAP PEPTIDE (60-100) AND MYRISTOATE (COVALENTLY BOUND) AT 2.1A (P41212 CRYSTAL FORM)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-06-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 59.096, 59.096, 158.949 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.550 - 2.100 |
R-factor | 0.233 |
Rwork | 0.232 |
R-free | 0.25290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kys |
RMSD bond length | 0.008 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.550 | 2.154 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.081 | 0.697 |
Rmeas | 0.084 | 0.727 |
Rpim | 0.084 | 0.471 |
Number of reflections | 17209 | |
<I/σ(I)> | 22.9 | 4.2 |
Completeness [%] | 99.8 | 100 |
Redundancy | 12.6 | 12.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | 16% PEG 3350,2% tacsimate, 0.1M NaCit |