6PQ0

LCP-embedded Proteinase K treated with MPD

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	67.340, 67.340, 106.475
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	17.390 - 2.000
R-factor	0.2218
Rwork	0.217
R-free	0.26650
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2id8
RMSD bond length	0.003
RMSD bond angle	0.571
Data reduction software	iMOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]		2.072
High resolution limit [Å]	2.000	2.000
Number of reflections		782
<I/σ(I)>		3.4
Completeness [%]		63
Redundancy		6.3
CC(1/2)		0.368