6PLK
Crystal structure of ZIKV-116 Fab in complex with ZIKV envelope DIII
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-11-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.809, 89.805, 92.487 |
Unit cell angles | 90.00, 103.96, 90.00 |
Refinement procedure
Resolution | 44.903 - 2.300 |
R-factor | 0.1696 |
Rwork | 0.167 |
R-free | 0.21070 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5KVG and 5GZO |
RMSD bond length | 0.004 |
RMSD bond angle | 0.656 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.344 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 50016 | 2471 |
<I/σ(I)> | 22.5 | |
Completeness [%] | 97.5 | |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 30% MPD, 0.1 M Imidazole and 10% PEG 4K |