6PL2
TRK-A IN COMPLEX WITH LIGAND 1a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 52.080, 52.080, 226.964 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.000 - 2.590 |
R-factor | 0.20155 |
Rwork | 0.196 |
R-free | 0.27414 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.226 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.660 | 2.840 |
High resolution limit [Å] | 2.590 | 2.590 |
Rmerge | 0.730 | 0.435 |
Number of reflections | 11318 | |
<I/σ(I)> | 17.96 | |
Completeness [%] | 99.6 | 98.8 |
Redundancy | 4.7 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 20mM Tris/HCl |