6PGA
WDR5delta32 bound to methyl (4-(4-(hydroxymethyl)-1H-imidazol-2-yl)butyl)carbamate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-08-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.782, 64.991, 97.386 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.170 - 2.450 |
R-factor | 0.19942 |
Rwork | 0.197 |
R-free | 0.25028 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6pg4 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.390 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.170 | 2.550 |
High resolution limit [Å] | 2.450 | 2.450 |
Number of reflections | 11445 | 1242 |
<I/σ(I)> | 5.9 | 2 |
Completeness [%] | 99.9 | 99.4 |
Redundancy | 12.4 | 12.8 |
CC(1/2) | 0.980 | 0.762 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 281 | 0.237 M ammonium sulfate, 0.1 M bis-tris chloride, 25.7 %w/v MPEG5000 |