6P96
OXA-48 carbapanemase, apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.746, 76.827, 100.044 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.413 - 1.600 |
R-factor | 0.185 |
Rwork | 0.184 |
R-free | 0.20890 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.413 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 72537 | 3522 |
<I/σ(I)> | 13.8 | 1.7 |
Completeness [%] | 99.9 | 99.2 |
Redundancy | 13.1 | 12.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 5 mM Ca2+, 5 mM Co2+, 5 mM Cd2+, 20% PEG 3350 |