6OM8
Caenorhabditis Elegans UDP-Glucose Dehydrogenase in complex with UDP-Xylose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2017-06-21 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 1.0 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 157.710, 168.170, 279.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.698 - 2.449 |
R-factor | 0.1937 |
Rwork | 0.194 |
R-free | 0.22040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2o3j |
RMSD bond length | 0.008 |
RMSD bond angle | 0.911 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.698 | 2.510 |
High resolution limit [Å] | 2.449 | 2.449 |
Number of reflections | 266791 | 19914 |
<I/σ(I)> | 9.1 | |
Completeness [%] | 98.1 | |
Redundancy | 6.295 | |
CC(1/2) | 0.996 | 0.455 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 10 mg/mL C. Elegans UDP-Glucose Dehydrogenase Citric acid buffer pH 5.0 200mM Lithium Chloride 4% PEG 8000 |