6OM1
Crystal structure of an atypical integrin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2017-10-29 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 1 |
Unit cell lengths | 144.240, 55.070, 175.070 |
Unit cell angles | 90.37, 107.00, 90.01 |
Refinement procedure
Resolution | 48.072 - 2.660 |
R-factor | 0.2486 |
Rwork | 0.248 |
R-free | 0.27960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4um9 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.736 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.072 | 2.730 |
High resolution limit [Å] | 2.660 | 2.660 |
Rmerge | 0.094 | |
Rmeas | 0.133 | |
Number of reflections | 141394 | 10550 |
<I/σ(I)> | 5.87 | |
Completeness [%] | 95.5 | 96.8 |
Redundancy | 1.7 | 1.7 |
CC(1/2) | 0.994 | 0.199 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 277 | 100 mM MES, pH 6.7, 12% PEG 20000 |