6OCO
HUMAN PI3KDELTA IN COMPLEX WITH COMPOUND 6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 91.017, 108.981, 142.394 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 86.540 - 2.580 |
R-factor | 0.2596 |
Rwork | 0.259 |
R-free | 0.29600 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | NONE |
RMSD bond length | 0.008 |
RMSD bond angle | 1.022 |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.540 | 2.830 |
High resolution limit [Å] | 2.580 | 2.580 |
Rmerge | 0.064 | 0.541 |
Rmeas | 0.068 | 0.578 |
Number of reflections | 45261 | 201 |
<I/σ(I)> | 18.9 | 4.28 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 8.2 | 8.2 |
CC(1/2) | 0.998 | 0.992 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 16.60 % PEG6000 0.10 M KCl 0.10 M MES pH=6.00 |