6OBZ
Crystal structure of FluA-20 Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2016-08-19 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.03319 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 83.577, 52.643, 104.786 |
Unit cell angles | 90.00, 93.77, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.730 |
R-factor | 0.2039 |
Rwork | 0.202 |
R-free | 0.23810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4kmt 5bv7 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.929 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.760 |
High resolution limit [Å] | 1.730 | 1.730 |
Rpim | 0.050 | 0.210 |
Number of reflections | 92959 | 4414 |
<I/σ(I)> | 11.8 | |
Completeness [%] | 97.8 | 93.6 |
Redundancy | 3.5 | 3.2 |
CC(1/2) | 1.000 | 0.840 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 0.2 M tri-sodium citrate 20% (w/v) PEG3350 |