6NWV
Insulin Lispro Analog
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.95 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.161, 61.789, 58.618 |
Unit cell angles | 90.00, 111.46, 90.00 |
Refinement procedure
Resolution | 42.960 - 1.601 |
R-factor | 0.21318 |
Rwork | 0.208 |
R-free | 0.25673 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ev6 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.409 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.960 | 1.690 |
High resolution limit [Å] | 1.601 | 1.600 |
Rmerge | 0.101 | 1.856 |
Rpim | 0.042 | 0.781 |
Number of reflections | 40488 | 4189 |
<I/σ(I)> | 10.4 | |
Completeness [%] | 99.7 | |
Redundancy | 6.8 | |
CC(1/2) | 0.375 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.1 M HEPES sodium pH 7.5; 0.4 M Potassium sodium tartrate tetrahydrate. |