6NSP
TRK-A IN COMPLEX WITH LIGAND 9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 51.994, 51.994, 228.163 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.070 - 2.310 |
R-factor | 0.1924 |
Rwork | 0.187 |
R-free | 0.25498 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.898 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.050 | 2.560 |
High resolution limit [Å] | 2.310 | 2.310 |
Number of reflections | 15796 | 15796 |
<I/σ(I)> | 19.45 | |
Completeness [%] | 98.7 | 97.2 |
Redundancy | 4.1 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1M KH2PO4/ 0.1M NaH2PO4/ 0.1M MES/NaOH pH 6.0 and 1.9M NaCl (cryo: 25% glycerol in reservoir), or 18% (w/v) PEG 3350, 0.2M CaCl2, 0.1M, MES pH = 6.50 (cryo: direct). |