6NKO

Crystal structure of ForH

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-B
Synchrotron site	APS
Beamline	23-ID-B
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-05-22
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.0332
Spacegroup name	P 2 21 21
Unit cell lengths	57.218, 111.401, 163.396
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.930 - 2.403
R-factor	0.2142
Rwork	0.212
R-free	0.26160
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1m9n
RMSD bond length	0.004
RMSD bond angle	0.634
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.440
High resolution limit [Å]	2.400	2.400
Number of reflections	41344	4551
<I/σ(I)>	15.14
Completeness [%]	100.0
Redundancy	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	2 M ammonium sulfate, 0.1 M Bis-Tris, pH 5.5