6NJI

Crystal Structure of the PDE4D Catalytic Domain and UCR2 Regulatory Helix with T-49

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.45 Å)

Cell axes124.04085.66083.450
Cell angles90.00110.4190.00
SpacegroupC 1 2 1
Resolution limits42.87 - 2.45
the highest resolution shell value2.510 - 2.450
R-factor0.187
R-work0.18400
the highest resolution shell value0.264
R-free0.23000
the highest resolution shell value0.337
RMSD bond length0.014
RMSD bond angle1.534

Data Collection Statistics

Resolution limits50.00 - 2.45
the highest resolution shell value -
Number of reflections29617
Rmerge_l_obs0.046
the highest resolution shell value0.504
Completeness97.9
Redundancy3.3
the highest resolution shell value3.3
I/sigma(I)-3

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, SITTING DROP7.147.14289

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*