6N9O
Crystal structure of human GSDMD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-22 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.640, 105.550, 151.790 |
Unit cell angles | 90.00, 94.47, 90.00 |
Refinement procedure
Resolution | 49.483 - 3.500 |
R-factor | 0.2796 |
Rwork | 0.276 |
R-free | 0.34540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5b5r 6ao3 6ao4 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.891 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX ((1.14_3260: ???)) |
Refinement software | PHENIX ((1.15.2_3472: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.500 | 3.600 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmeas | 0.086 | |
Number of reflections | 23251 | 1695 |
<I/σ(I)> | 10.2 | 1.4 |
Completeness [%] | 99.1 | 99.3 |
Redundancy | 3.2 | |
CC(1/2) | 0.997 | 0.605 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 25% PEG3350, 0.1M Bis-Tris pH 5.5, 200 mM NaCl, and 10 mM DTT |