6N8P
Crystal structure of the human cell polarity protein Lethal Giant Larvae 2 (Lgl2). Unphosphorylated, crystal form 1.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-07-25 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0055 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.699, 118.489, 126.639 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.349 - 3.193 |
R-factor | 0.2081 |
Rwork | 0.204 |
R-free | 0.24970 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.479 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.350 | 3.410 |
High resolution limit [Å] | 3.190 | 3.190 |
Rmerge | 0.419 | 2.097 |
Number of reflections | 20282 | 3625 |
<I/σ(I)> | 5.9 | 1.7 |
Completeness [%] | 99.8 | 99.5 |
Redundancy | 6.5 | 6.8 |
CC(1/2) | 0.972 | 0.495 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295.15 | 19.8 % PEG 3350, 0.29 M Na2SO4, 0.1 M bis-tris propane pH 7.5, 3% methanol |