6N64
Crystal structure of mouse SMCHD1 hinge domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-11 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 123.549, 123.549, 232.869 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.450 - 3.300 |
R-factor | 0.206 |
Rwork | 0.204 |
R-free | 0.23900 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.160 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.450 | 3.418 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmeas | 0.205 | 1.956 |
Rpim | 0.048 | 0.461 |
Number of reflections | 27936 | 2722 |
<I/σ(I)> | 14.81 | 2.03 |
Completeness [%] | 99.9 | 99.71 |
Redundancy | 17.7 | 17.9 |
CC(1/2) | 0.999 | 0.674 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 9.35 | 281 | 0.1 M Sodium Bicine pH 9.35, 0.18 M MgCl2, 20% (v/v) 2-propanol |