6MU4
Bst DNA polymerase I FANA/DNA binary complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-21 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 87.835, 93.898, 105.809 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.092 - 1.620 |
R-factor | 0.1878 |
Rwork | 0.187 |
R-free | 0.21050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l3s |
RMSD bond length | 0.006 |
RMSD bond angle | 0.936 |
Data reduction software | autoXDS |
Data scaling software | autoXDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.092 | 1.670 |
High resolution limit [Å] | 1.620 | 1.620 |
Rmerge | 0.041 | 0.846 |
Number of reflections | 111377 | |
<I/σ(I)> | 23.32 | 2.22 |
Completeness [%] | 99.7 | |
Redundancy | 6.6 | |
CC(1/2) | 1.000 | 0.824 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 50% ammonium sulfate, 0.1M MES, 2% MPD |