6MQC
Vaccine-elicited NHP FP-targeting neutralizing antibody 0PV-c.01 in complex with FP (residue 512-519)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.122, 72.898, 169.305 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.625 - 1.990 |
R-factor | 0.2005 |
Rwork | 0.199 |
R-free | 0.23370 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.053 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.111 | 0.064 | 0.808 |
Rmeas | 0.122 | 0.071 | 0.896 |
Rpim | 0.050 | 0.030 | 0.381 |
Total number of observations | 358892 | ||
Number of reflections | 62096 | 3358 | 3105 |
<I/σ(I)> | 6.1 | ||
Completeness [%] | 99.6 | 99.2 | 99.9 |
Redundancy | 5.8 | 5.3 | 5.1 |
CC(1/2) | 0.995 | 0.792 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M NaNO3 and 20% w/v PEG 3350 |