6MOK
Dimeric DARPin A_distance_R7 complex with EpoR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-04-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00001 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 117.090, 117.090, 233.587 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.790 - 5.101 |
R-factor | 0.23254 |
Rwork | 0.225 |
R-free | 0.29890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | predicted model 1ern |
RMSD bond length | 0.006 |
RMSD bond angle | 1.443 |
Data reduction software | XDS (Jan 26, 2018) |
Data scaling software | XDS (Jan 26, 2018) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.790 | 5.283 |
High resolution limit [Å] | 5.101 | 5.101 |
Rmerge | 0.116 | 2.750 |
Rmeas | 0.123 | |
Rpim | 0.039 | 0.884 |
Number of reflections | 4205 | 395 |
<I/σ(I)> | 9.92 | 0.9 |
Completeness [%] | 98.4 | 98.74 |
Redundancy | 9.8 | 10.4 |
CC(1/2) | 0.996 | 0.585 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 295 | 0.2 M NaCl, 0.1 M Tris pH 8.5, 25% PEG 3350 |