6MKZ
Crystal structure of murine 4-1BB/4-1BBL complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.499, 88.478, 155.158 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 76.859 | 76.859 | 2.688 |
High resolution limit [Å] | 2.624 | 7.354 | 2.624 |
Total number of observations | 349768 | 15728 | 9414 |
Number of reflections | 25447 | 1306 | 1263 |
<I/σ(I)> | 5.6 | 7.8 | 1.7 |
Completeness [%] | 97.6 | 99.8 | 71 |
Redundancy | 13.7 | 12 | 7.5 |
CC(1/2) | 0.960 | 0.949 | 0.755 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 20% PEG 4000, 0.2M ammonium chloride |