6MFF

HLA-DQ2-glia-omega1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	CCD
Collection date	2017-06-14
Detector	ADSC QUANTUM 210r
Wavelength(s)	0.9537
Spacegroup name	C 2 2 21
Unit cell lengths	93.870, 96.610, 107.050
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.935 - 2.600
R-factor	0.2107
Rwork	0.209
R-free	0.25030
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.575
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	67.320	2.740
High resolution limit [Å]	2.600	2.600
Rpim	0.044	0.366
Number of reflections	15331	2200
<I/σ(I)>	13.4	2.3
Completeness [%]	100.0	100
Redundancy	12.5	12.7
CC(1/2)	0.998	0.719

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	23% PEG3350 and 0.1 M NaH2PO4, pH 6