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6M3B

hAPC-c25k23 Fab complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U1
Synchrotron siteSSRF
BeamlineBL17U1
Temperature [K]100
Detector technologyCCD
Collection date2012-04-21
DetectorADSC QUANTUM 315r
Wavelength(s)1
Spacegroup nameC 1 2 1
Unit cell lengths112.277, 94.889, 114.320
Unit cell angles90.00, 105.49, 90.00
Refinement procedure
Resolution27.542 - 2.200
R-factor0.2198
Rwork0.218
R-free0.24750
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1aut
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX (1.15.2_3472)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.260
High resolution limit [Å]2.2002.200
Rmerge0.0960.989
Rpim0.531
Number of reflections570994288
<I/σ(I)>32.223.04
Completeness [%]97.2
Redundancy4.2
CC(1/2)0.9910.825
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2910.1% n-Octyl-beta-D-glucoside, 0.1M sodium citrate tribasic dehydrate pH 5.5, 22% (w/v) PEG 3350

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