6M31
Structural and Functional Insights into an Archaeal Lipid Synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-10 |
Detector | DECTRIS PILATUS3 R 1M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.000, 133.490, 79.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.890 - 2.300 |
R-factor | 0.202 |
Rwork | 0.201 |
R-free | 0.23000 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | SHELX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.890 | 3.970 | 2.430 |
High resolution limit [Å] | 2.290 | 3.440 | 2.290 |
Rmerge | 0.092 | 0.072 | 0.773 |
Rmeas | 0.099 | 0.078 | 0.834 |
Number of reflections | 33780 | 6618 | 10285 |
<I/σ(I)> | 13.4 | 2.63 | |
Completeness [%] | 99.8 | 100 | 99.5 |
Redundancy | 6.904 | 6.962 | 6.974 |
CC(1/2) | 0.999 | 0.999 | 0.930 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293.15 | 200 mM NaCl, 20% (w/v) PEG500, and 200 mM Tris-HCl (pH 8.0). |