6LZ9
t8E4 antibody Fab complexed with the active form of HGF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-27 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 176.180, 176.180, 122.960 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.970 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 28218 | 4412 |
<I/σ(I)> | 13.8 | |
Completeness [%] | 99.7 | |
Redundancy | 9.9 | |
CC(1/2) | 0.998 | 0.673 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 10 % (w/v) PEG 10000, 0.1M Magnesium acetate, 0.1M MES pH 6.5 |