6LCA
Crystal structure of human Dishevelled1 PDZ domain homotrimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | H 3 |
Unit cell lengths | 147.923, 147.923, 78.999 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.330 - 2.400 |
R-factor | 0.2464 |
Rwork | 0.245 |
R-free | 0.27270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fy5 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.536 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.550 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 25203 | 4095 |
<I/σ(I)> | 14.3 | 1.65 |
Completeness [%] | 99.9 | 98.8 |
Redundancy | 5 | 5.2 |
CC(1/2) | 0.999 | 0.743 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 0.5 M Ammonium sulfate 0.1 M Sodium citrate tribasic dehydrate 1.0 M Lithium sulfate monohydrate 0.01 M GSH 0.01 M GSSG |