6KY4
Crystal structure of Sulfiredoxin from Arabidopsis thaliana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 43 3 2 |
Unit cell lengths | 102.544, 102.544, 102.544 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.863 - 3.200 |
R-factor | 0.2492 |
Rwork | 0.244 |
R-free | 0.29380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xw3 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.310 |
High resolution limit [Å] | 3.200 | 6.890 | 3.200 |
Rmerge | 0.098 | 0.073 | 2.261 |
Rmeas | 0.099 | 0.074 | 2.292 |
Rpim | 0.018 | 0.015 | 0.372 |
Total number of observations | 124863 | ||
Number of reflections | 3377 | 395 | 330 |
<I/σ(I)> | 12 | ||
Completeness [%] | 99.9 | 99 | 100 |
Redundancy | 37 | 24.9 | 37.2 |
CC(1/2) | 0.998 | 0.851 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 289 | 0.8 M NaH2PO4/1.2 M KH2PO4, acetate pH 4.5 |