6KQB
A long chain secondary alcohol dehydrogenase of Micrococcus luteus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 64.492, 64.492, 321.543 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.530 - 2.261 |
R-factor | 0.2175 |
Rwork | 0.215 |
R-free | 0.25960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4dyd |
RMSD bond length | 0.008 |
RMSD bond angle | 0.858 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.300 |
High resolution limit [Å] | 2.260 | 2.260 |
Rmeas | 0.189 | 0.987 |
Number of reflections | 37786 | 1861 |
<I/σ(I)> | 11.4 | |
Completeness [%] | 99.9 | |
Redundancy | 17.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294.15 | Sodium citrate tribasic dihydrate |