6KIJ
Crystal structure of yedK with ssDNA containing an abasic site
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-01-08 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.444, 44.080, 55.148 |
Unit cell angles | 90.00, 102.33, 90.00 |
Refinement procedure
Resolution | 23.170 - 1.580 |
R-factor | 0.154 |
Rwork | 0.152 |
R-free | 0.18300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6kbs |
RMSD bond length | 0.006 |
RMSD bond angle | 0.901 |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.640 |
High resolution limit [Å] | 1.579 | 1.580 |
Rmerge | 0.121 | 0.689 |
Number of reflections | 30514 | 2980 |
<I/σ(I)> | 4 | |
Completeness [%] | 99.3 | 98.4 |
Redundancy | 6.7 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 293 | 0.2M Ammonium formate 20% w/v PEG3350 |