Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

6K5K

Structural and catalytic analysis of two diverse uridine phosphorylases in the oomycete Phytophthora capsici.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL19U1
Synchrotron siteSSRF
BeamlineBL19U1
Temperature [K]100
Detector technologyPIXEL
Collection date2018-09-12
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.97
Spacegroup nameP 2 21 21
Unit cell lengths66.790, 97.382, 188.520
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution48.691 - 2.097
R-factor0.2497
Rwork0.246
R-free0.31700
Structure solution methodSAD
Data reduction softwareHKL-3000
Data scaling softwareHKL-3000
Phasing softwareSOLVE
Refinement softwarePHENIX (1.13_2998)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.140
High resolution limit [Å]2.0902.090
Number of reflections725437120
<I/σ(I)>16.9
Completeness [%]99.9
Redundancy13.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP62830.1M sodium citrate tribasic dihydrate PH 5.0, 22% PEG 1000

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon