6K3E
LSD1/Co-Rest structure with an inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 121.510, 179.440, 234.410 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 76.460 - 2.870 |
R-factor | 0.19028 |
Rwork | 0.189 |
R-free | 0.22282 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5h6q |
RMSD bond length | 0.011 |
RMSD bond angle | 1.909 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 76.460 | 76.340 | 2.940 |
High resolution limit [Å] | 2.870 | 12.840 | 2.870 |
Rmerge | 0.080 | 0.049 | 1.064 |
Number of reflections | 58422 | 736 | 4288 |
<I/σ(I)> | 13.5 | ||
Completeness [%] | 99.4 | 98.9 | 99.7 |
Redundancy | 6.8 | 6.1 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 36% Tacsimate |