6JX5
Hect domain of AREL1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 296 |
Detector technology | PIXEL |
Collection date | 2018-04-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9926 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 209.156, 121.057, 80.798 |
Unit cell angles | 90.00, 91.49, 90.00 |
Refinement procedure
Resolution | 47.860 - 2.402 |
R-factor | 0.1873 |
Rwork | 0.186 |
R-free | 0.21810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3tug |
RMSD bond length | 0.003 |
RMSD bond angle | 0.627 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.860 | 2.488 |
High resolution limit [Å] | 2.400 | 2.402 |
Rpim | 0.049 | 0.235 |
Number of reflections | 77372 | 7296 |
<I/σ(I)> | 19.22 | |
Completeness [%] | 98.7 | |
Redundancy | 5.7 | |
CC(1/2) | 0.993 | 0.832 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 296.15 | 100mM Bis Tris (pH 5.5), 200mM Ammonium sulfate |