6JVX
Crystal structure of RBM38 in complex with RNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 78.809, 78.809, 66.982 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.405 - 2.301 |
R-factor | 0.1795 |
Rwork | 0.177 |
R-free | 0.22050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2cqd |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.380 |
High resolution limit [Å] | 2.300 | 4.950 | 2.300 |
Rmerge | 0.101 | 0.058 | 0.942 |
Rmeas | 0.113 | 0.065 | 1.057 |
Rpim | 0.049 | 0.028 | 0.468 |
Total number of observations | 53598 | ||
Number of reflections | 10894 | 1151 | 1075 |
<I/σ(I)> | 9.8 | ||
Completeness [%] | 98.9 | 97.1 | 99.1 |
Redundancy | 4.9 | 4.6 | 5 |
CC(1/2) | 0.996 | 0.679 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 289 | 0.1M Tris-HCl (pH8.0), 2M ammonium sulfate |