Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

6JUZ

Crystal Structure of N-terminal domain of ArgZ(N71S) covalently bond to a reaction intermediate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U1
Synchrotron siteSSRF
BeamlineBL17U1
Temperature [K]100
Detector technologyPIXEL
Collection date2018-04-29
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.97916
Spacegroup nameP 1 21 1
Unit cell lengths40.530, 87.549, 43.196
Unit cell angles90.00, 93.74, 90.00
Refinement procedure
Resolution25.026 - 1.210
R-factor0.1661
Rwork0.166
R-free0.17540
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)6jv0
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX (1.14_3260)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0001.230
High resolution limit [Å]1.2103.2801.210
Rmerge0.0540.0420.489
Rmeas0.0610.0480.564
Rpim0.0270.0220.276
Number of reflections8971344354456
<I/σ(I)>18.3
Completeness [%]98.295.197.2
Redundancy4.84.83.8
CC(1/2)0.9930.804
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52950.2 M KI, 0.1 M MES pH 6.5, 19% PEG 4000

227344

PDB entries from 2024-11-13

PDB statisticsPDBj update infoContact PDBjnumon