6JQ6
Hatchet Ribozyme Structure soaking with Ir(NH3)6+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-02 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.103 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 91.830, 91.830, 140.627 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.626 |
R-factor | 0.1996 |
Rwork | 0.196 |
R-free | 0.22930 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.236 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.720 |
High resolution limit [Å] | 2.610 | 2.610 |
Rpim | 0.041 | 2.290 |
Number of reflections | 19049 | 683 |
<I/σ(I)> | 20.2 | |
Completeness [%] | 99.0 | |
Redundancy | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.20M K-formate, 2.2M (NH4)2SO4 |