6JOD
Angiotensin II type 2 receptor with ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-05-22 |
Detector | RAYONIX MX225-HS |
Wavelength(s) | 1 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 102.550, 426.430, 52.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.854 | 3.310 |
High resolution limit [Å] | 3.200 | 3.200 |
Rpim | 0.050 | 0.551 |
Number of reflections | 19767 | 1933 |
<I/σ(I)> | 17.47 | |
Completeness [%] | 99.9 | |
Redundancy | 82.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293 | 30% (v/v) PEG 300 0.1 M HEPES (pH 7.0) 100 mM Sodium phosphate dibasic dihydrate |