6JO0
Crystal structure of the DTS-motif rhodopsin from Phaeocystis globosa virus 12T
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-08 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 45.194, 57.832, 117.037 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.160 - 1.651 |
R-factor | 0.1926 |
Rwork | 0.192 |
R-free | 0.20900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5b2n |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 45.190 | 45.190 | 1.680 |
High resolution limit [Å] | 1.650 | 9.040 | 1.650 |
Rmerge | 0.086 | 0.046 | 1.628 |
Rmeas | 0.094 | 0.051 | 1.767 |
Rpim | 0.036 | 0.022 | 0.678 |
Number of reflections | 37658 | 284 | 1819 |
<I/σ(I)> | 10.2 | ||
Completeness [%] | 99.9 | 98.9 | 99 |
Redundancy | 6.6 | 5.5 | 6.6 |
CC(1/2) | 0.998 | 0.996 | 0.603 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 5.5 | 293 | Na-citrate (pH 5.5), 150 mM Na-phosphate, 25% PEG 600 |