6J1X
WWP1 close conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-04-07 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.309, 45.444, 116.545 |
Unit cell angles | 90.00, 93.79, 90.00 |
Refinement procedure
Resolution | 35.810 - 2.300 |
R-factor | 0.2221 |
Rwork | 0.220 |
R-free | 0.27050 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xmc |
RMSD bond length | 0.007 |
RMSD bond angle | 0.830 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.290 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.070 | 0.360 |
Number of reflections | 26023 | 2599 |
<I/σ(I)> | 16.3 | 3 |
Completeness [%] | 97.7 | 97.7 |
Redundancy | 3.5 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | 100mM Tris-HCl pH 7.0, 15% v/v reagent alcohol |