6J0D

Crystal structure of OsSUF4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2018-04-07
Detector	ADSC QUANTUM 315
Wavelength(s)	0.97918
Spacegroup name	P 41 21 2
Unit cell lengths	74.024, 74.024, 37.577
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.340 - 1.900
R-factor	0.19749
Rwork	0.196
R-free	0.23022
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.020
RMSD bond angle	1.953
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	REFMAC (5.8.0158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.340	1.970
High resolution limit [Å]	1.900	1.900
Rmerge	0.136
Number of reflections	8598
<I/σ(I)>	24.7
Completeness [%]	99.9
Redundancy	10.3
CC(1/2)	0.998	0.831

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	Hepes pH7.0,PEG6000