6IUI
Crystal structure of GIT1 PBD domain in complex with Paxillin LD4 motif
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | I 4 |
Unit cell lengths | 128.803, 128.803, 47.644 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.201 - 2.600 |
R-factor | 0.1957 |
Rwork | 0.194 |
R-free | 0.22560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6iuh |
RMSD bond length | 0.002 |
RMSD bond angle | 0.521 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.640 |
High resolution limit [Å] | 2.600 | 7.050 | 2.600 |
Rmerge | 0.054 | 0.042 | 0.986 |
Rmeas | 0.059 | 0.047 | 1.065 |
Rpim | 0.023 | 0.019 | 0.401 |
Number of reflections | 12341 | 655 | 621 |
<I/σ(I)> | 7.1 | ||
Completeness [%] | 99.9 | 98.3 | 100 |
Redundancy | 6.7 | 6 | 7 |
CC(1/2) | 0.997 | 0.751 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.1M HEPES pH 7.5, 30% w/v PEG 1000 |