6IMJ
The crystal structure of Se-AsfvLIG:DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-06-01 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 94.828, 63.099, 119.265 |
Unit cell angles | 90.00, 89.93, 90.00 |
Refinement procedure
Resolution | 29.936 - 2.554 |
R-factor | 0.2245 |
Rwork | 0.223 |
R-free | 0.26080 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.765 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL2Map |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.640 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.135 | 0.576 |
Number of reflections | 44993 | 4370 |
<I/σ(I)> | 13.2 | 1.92 |
Completeness [%] | 97.7 | 95 |
Redundancy | 4.7 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 291 | 0.1 M BIS-TRIS pH 5.5, 15% w/v PEG 100000.1 M Ammonium acetate, 0.1 M Cadmium chloride |