6HZW
THE GLIC PENTAMERIC LIGAND-GATED ION CHANNEL 2.22 resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 191 |
Detector technology | PIXEL |
Collection date | 2015-10-11 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9771 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 182.416, 133.401, 160.474 |
Unit cell angles | 90.00, 102.48, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.220 |
R-factor | 0.1965 |
Rwork | 0.195 |
R-free | 0.22009 |
RMSD bond length | 0.019 |
RMSD bond angle | 2.234 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.390 | 2.260 |
High resolution limit [Å] | 2.220 | 2.220 |
Number of reflections | 169456 | |
<I/σ(I)> | 8.7 | |
Completeness [%] | 91.9 | |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 291 | 12-14.5% PEG4K; 15% GLycerol; 400 mM NaSCN; 3% DMSO; 100mM NaAcetate pH 4. |