6HX2

The structure of Dps from Listeria innocua soaked with Cobalt

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-10-11
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	1
Spacegroup name	P 41 21 2
Unit cell lengths	87.581, 87.581, 277.363
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.045 - 1.597
R-factor	0.1556
Rwork	0.155
R-free	0.17110
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.766
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	1.690
High resolution limit [Å]	1.597	1.600
Number of reflections	272612
<I/σ(I)>	12.87
Completeness [%]	99.8
Redundancy	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	298	20% PEG3350